One-Pot Synthesis of Copper Iodide-Polypyrrole Nanocomposites
نویسندگان
چکیده
A novel one-pot chemical synthesis of functional copper iodide-polypyrrole composites, CuI-PPy, has been proposed. The fabrication process allows the formation nanodimensional metal salt/polymer hybrid structures in a fully controlled time- and concentration-dependent manner. impact certain experimental conditions, viz., duration synthesis, sequence component addition concentrations intact reagents on structure, dimensionality yield end-product was evaluated detail. More specifically, amount marshite CuI within composite can be ranged from 60 to 90 wt.%, depending synthetic conditions (type concentration components, duration). In addition, allowing nano-sized distributed inside polypyrrole matrix were found. high morphological stability reproducibility synthesized metal-polymer materials approved. Finally, electrochemical activity formed composites verified by cyclic voltammetry studies. CuI-PPy deposited electrodes strongly affected applied anodic limit. proposed is highly innovative, meets requirements Green Chemistry potentially useful for future biosensor development. this study expected generally contribute knowledge nano-based with tailored properties.
منابع مشابه
Nanocrystalline copper(II) oxide-catalyzed one-pot four- component synthesis of polyhydroquinoline derivativesunder solvent-free conditions
The efficient and environmentally friendly method for the one-pot synthesis of polyhydroquinolines has been developed in the presence of CuO nanoparticles. The multi-component reactions of aldehydes, dimedone, ethyl acetoacetate andammonium acetate were carried out under solvent-free conditions to afford some polyhydroquinoline derivatives. This method provides several advantages including high...
متن کاملPot economy and one-pot synthesis
The one-pot synthesis of a target molecule in the same reaction vessel is widely considered to be an efficient approach in synthetic organic chemistry. In this review, the characteristics and limitations of various one-pot syntheses of biologically active molecules are explained, primarily involving organocatalytic methods as key tactics. Besides catalysis, the pot-economy concepts presented he...
متن کاملOne-pot Synthesis of Polysubstituted Indolizine Derivatives
An efficient approach to the synthesis of 1,2,3-trisubstituted indolizines is described via one-pot reactions of pyridine and dialkyl acetylendicarboxylate in the presence of ethyl 2-chloroacetoacetate in MeOH at room temperature. The corresponding 1, 2, 3-trisubstituted indolizines may be useful building blocks for the construction of complex indolizine derivatives.
متن کاملA Modified-One Pot Synthesis of Diaminoglyoxime
The one pot reaction of glyoxal and hydroxylamine hydrochloride in aqueous sodium hydroxide was found to be a safe and inexpensive method for the preparation of diaminoglyoxime. By increasing stoichiometric ratio of the hydroxylamine hydrochloride and decreasing the solvent volume, the product yield increased considerably (~ 70%).
متن کاملOne-pot synthesis of (−)-Ambrox
(-)-Ambrox is recognised as the prototype of all ambergris odorants. Widely used in perfumery, (-)-Ambrox is an important ingredient due to its unique scent and excellent fixative function. An environmentally friendly and practical preparation of (-)-Ambrox is still unavailable at present although a lot of attention has been paid to this hot research topic for many years. A one-pot synthesis of...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Chemosensors
سال: 2021
ISSN: ['2227-9040']
DOI: https://doi.org/10.3390/chemosensors9030056